Ceramic vessel 8-J. Oppidum of Puente Tablas (Jaén, Spain)

Ceramic vessel 8-J from space J of the Sanctuary of the Iberian oppidum in Puente Tablas (Jaén, Spain).Wheelmade ceramic, oxidising firing. It has no decoration. The analysis of contents was carried out using GC-MS obtaining the peak of native sulphur (S8). The presence of sulphur in this ritual context is related to ceremonies for the purification of objects, spaces and atmospheres.

Condition: New product

Dimensions

Ancho : 14.5 Centimeters

Alto : 12 Centimeters

Materials

pottery

Temporal

Period name : Iberian

Date : Early 4th BC

Spatial

Location : Oppidum de Puente Tablas

Geopolitical area : Puente Tablas, Jaén, Spain

Spatial reference system : WGS84

Copyrights

Creative Commons - Attribution, Non-Commercial, No Derivatives (BY-NC-ND)

References

Article - Parras, D., Sánchez, A., Tuñón, J., Rueda, C., Ramos, N. García-Reyes, J.F. (2015): “Sulphur, fats and beeswax in the Iberian rites of the sanctuary of the oppidum of Puente Tablas (Jaén, Spain)”. Journal of Archaeological Science: Reports, 4: 510-524.

Digital Resources

Ceramic vessel 8-J Instituto Universitario de Investigación en Arqueología Ibérica. Universidad de Jaén

Creative Commons - Attribution, Non-Commercial, No Derivatives (BY-NC-ND)
Arquiberlab
http://creativecommons.org/licenses/by-nc-nd/3.0/
Aerial view. Oppidum of Puente Tablas Instituto Universitario de Investigación en Arqueología Ibérica. Universidad de Jaén

Creative Commons - Attribution, Non-Commercial, No Derivatives (BY-NC-ND)
Arquiberlab
http://creativecommons.org/licenses/by-nc-nd/3.0/
Orthophoto. Sanctuary of Puente Tablas Instituto Universitario de Investigación en Arqueología Ibérica. Universidad de Jaén

Creative Commons - Attribution, Non-Commercial, No Derivatives (BY-NC-ND)
Arquiberlab
http://creativecommons.org/licenses/by-nc-nd/3.0/
GC-MS of sulphur Instituto Universitario de Investigación en Arqueología Ibérica. Universidad de jaén

Creative Commons - Attribution, Non-Commercial, No Derivatives (BY-NC-ND)
Arquiberlab
http://creativecommons.org/licenses/by-nc-nd/3.0/

Activities

Archaeometric analysis

Chromatographic analysis and structural determination

Pottery. Analysis of contents

Gass Chromatography-Mass Spectrometry

Content analysis

Destructive method for the identification of the total lipid profile: fatty acids, sterols, wax esters, fatty alcohols, triacylglycerols, etc. Any remains of soil were removed with an electric hand-drill. The sample was then grinded to the appropriate size in an agatha mortar (0.25 mm). Extraction with a mixture chloroform/methanol (CHCl3:MeOH) (2:1 v/v) assisted by ultrasound. Derivatization of lipids to trimethylsilyl derivatives (TMS). The reaction takes place at 70 ° C for 30 min using N,O-bis- (trimethylsilyl) trifluoroacetamide (BSTFA), with 1% trimethylchlorosilane (TMCS). The sample is solved in cyclohexane and then injected in GC-MS. Chromatographic separation is performed applying a adequate temperature program.

The analyses were performed using a using a gas chromatography equipment (model Thermo TraceGC Ultra) coupled to a Thermo DC Q II mass spectrometer. Autosampler Thermo Triplus (CICT, University of Jaén). The samples were introduced by on-column injection into a 15 m x 0.25 mm I.D. fused silica capillary column, coated with poly(dimethylsiloxane) stationary phase with 0.1 μm film thickness. Helium was used as the carrier gas (purity 99.99%).